Comparative SEM and TEM analyses of apatite phases
For characterizing each apatite phases based on light elements such as C, N, O, and F, SEM-EDS analysis was carried out in 5 kV and the representative EDS spectra are shown in Fig. 2. Ca peaks in all apatite phases are low because of the low Ca signal yield in 5 kV. Therefore, Ca/P ratio values were obtained in 15 kV. The carbon film of the …
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